piwik-script

English Intern
Institut für Organische Chemie

Abteilung für NMR-Spektroskopie

Leiter

Dr. Matthias Grüne

Tel.: +49 931 31 85309
matthias.gruene@uni-wuerzburg.de

Lebenslauf und Publikationsliste

Technische Mitarbeiterin

Patricia Altenberger

Tel.: +49 931 31 88154
patricia.altenberger@uni-wuerzburg.de


Equipment

Bruker Avance III HD 600 (‘nmr600a‘)
Bruker Avance III HD 600 (nmr600a)

Bruker Avance III HD 600 (‘nmr600a‘)

  • Single bay, installation 2014
  • Oxford magnet, installation 1994
  • SampleXpress automatic sample changer
  • BCU 1 variable temperature precooling unit
  • Cryo platform
  • DCH 13C / 1H cryoprobe with z gradient and ATM
  • Cryofit flow insert for HPLC hyphenation, 120 µl active volume

Main applications:

  • 1D and 2D NMR experiments with high sensitivity (cryoprobe), 0 to 80 °C
  • HPLC-NMR hyphenation
Bruker Avance III HD 600 (‘nmr600b‘)
Bruker Avance III HD 600 (‘nmr600b‘)

Bruker Avance III HD 600 (‘nmr600b‘)

  • Double bay, installation 2014
  • Bruker Ascend magnet, installation 2014
  • BACS 120 automatic sample changer
  • BCU 2 variable temperature precooling unit for sample temperatures down to -55 °C
  • Liquid nitrogen heat exchanger for lowest sample temperatures
  • BBFO standard probe with z gradient and ATM, 15N to 31P + 19F / 1H, -150 to +150 °C
  • 10 mm 13C / 1H probe with z gradient and ATM, long term measurements up to 200 °C
  • Equipment for diffusion measurements with pulsed field gradients up to 1800 G/cm:
  • DIFF30L probe (1H inverse / 13C) and GREAT 60 A gradient amplifier
  • 3.2 mm MAS DVT probe, 15N to 31P / 1H + 19F
  • 1.3 mm MAS DVT probe, 15N to 31P + 14N / 1H + 19F

Main applications:         

  • 1D and 2D NMR experiments including heteronuclei
  • Variable temperature measurements
  • DOSY (i.a. large aggregates)
  • Solid state NMR (MAS)

Spare probes for 600 MHz (purchase before 2005):

  • BBO probe with z gradient and ATM, 15N to 31P / 1H
  • TXI probe (1H inverse / 13C / 15N) with z gradient, without ATM
  • Dual probe (19F / 1H) without gradient, without ATM
  • 10 mm BBO probe without gradient, without ATM, 109Ag to 31P / 1H
  • 3 mm inverse (1H / 13C) HPLC NMR probe (60 µl active volume) with z gradient, without ATM
  • 4 mm inverse (1H / 13C) HPLC NMR probe (120 µl active volume) without gradient, without ATM
Bruker Avance III HD 400 (‘nmr400a‘)
Bruker Avance III HD 400 (‘nmr400a‘)

Bruker Avance III HD 400 (‘nmr400a‘)

  • Nanobay, installation 2014
  • Bruker Ultrashield magnet, installation 2000
  • BACS 60 automatic sample changer
  • BCU 05 variable temperature precooling unit
  • BBFO standard probe with z gradient and ATM, 15N to 31P + 19F / 1H, -150 to +150 °C

Main application:

1D and 2D NMR experiments including heteronuclei
(automation with ICON-NMR software)

Bruker Avance III HD 400 (‘nmr400b‘)
Bruker Avance III HD 400 (‘nmr400b‘)

Bruker Avance III HD 400 (‘nmr400b‘)

  • Nanobay, installation 2013
  • Bruker Ascend magnet, installation 2013
  • BACS 120 automatic sample changer
  • BCU 2 variable temperature precooling unit for sample temperatures down to -60 °C
  • Liquid nitrogen heat exchanger for lowest sample temperatures
  • BBFO standard probe with z gradient and ATM, 15N to 31P + 19F / 1H, -150 to +150 °C

Main applications:         

  • 1D and 2D NMR experiments including heteronuclei
    (automation with ICON-NMR software)
  • Variable temperature measurements

Spare probe for 400 MHz (purchase 2001):

BBO with z gradient and ATM, 15N to 31P / 1H

Hinweis zum Datenschutz

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Hinweis zum Datenschutz

Mit 'OK' verlassen Sie die Seiten der Universität Würzburg und werden zu Twitter weitergeleitet. Informationen zu den dort erfassten Daten und deren Verarbeitung finden Sie in deren Datenschutzerklärung.

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Kontakt

Institut für Organische Chemie
Am Hubland
97074 Würzburg

Fax: +49 931 31-84606
E-Mail

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Hubland Süd, Geb. C1