NMR Spectroscopy

Equipment
![[Translate to Englisch:] Bruker Avance III HD 600 ('nmr600a') [Translate to Englisch:] Bruker Avance III HD 600 (nmr600a)](/fileadmin/_processed_/f/6/csm_nmr600a_75a7ce5ae3.jpg)
Bruker Avance III HD 600 (‘nmr600a‘)
- Single bay, installation 2014
- Oxford magnet, installation 1994
- SampleXpress automatic sample changer
- BCU 1 variable temperature precooling unit
- Cryo platform
- DCH 13C / 1H cryoprobe with z gradient and ATM
- Cryofit flow insert for HPLC hyphenation, 120 µl active volume
Main applications:
- 1D and 2D NMR experiments with high sensitivity (cryoprobe), 0 to 80 °C
- HPLC-NMR hyphenation
![[Translate to Englisch:] Bruker Avance III HD 600 (‘nmr600b‘) [Translate to Englisch:] Bruker Avance III HD 600 (‘nmr600b‘)](/fileadmin/_processed_/3/2/csm_nmr600b_fe40c18b22.jpg)
Bruker Avance III HD 600 (‘nmr600b‘)
- Double bay, installation 2014
- Bruker Ascend magnet, installation 2014
- BACS 120 automatic sample changer
- BCU 2 variable temperature precooling unit for sample temperatures down to -55 °C
- Liquid nitrogen heat exchanger for lowest sample temperatures
- BBFO standard probe with z gradient and ATM, 15N to 31P + 19F / 1H, -150 to +150 °C
- 10 mm 13C / 1H probe with z gradient and ATM, long term measurements up to 200 °C
- Equipment for diffusion measurements with pulsed field gradients up to 1800 G/cm:
- DIFF30L probe (1H inverse / 13C) and GREAT 60 A gradient amplifier
- 3.2 mm MAS DVT probe, 15N to 31P / 1H + 19F
- 1.3 mm MAS DVT probe, 15N to 31P + 14N / 1H + 19F
Main applications:
- 1D and 2D NMR experiments including heteronuclei
- Variable temperature measurements
- DOSY (i.a. large aggregates)
- Solid state NMR (MAS)
Spare probes for 600 MHz (purchase before 2005):
- BBO probe with z gradient and ATM, 15N to 31P / 1H
- TXI probe (1H inverse / 13C / 15N) with z gradient, without ATM
- Dual probe (19F / 1H) without gradient, without ATM
- 10 mm BBO probe without gradient, without ATM, 109Ag to 31P / 1H
- 3 mm inverse (1H / 13C) HPLC NMR probe (60 µl active volume) with z gradient, without ATM
- 4 mm inverse (1H / 13C) HPLC NMR probe (120 µl active volume) without gradient, without ATM
![[Translate to Englisch:] Bruker Avance III HD 400 (‘nmr400a‘) [Translate to Englisch:] Bruker Avance III HD 400 (‘nmr400a‘)](/fileadmin/_processed_/7/5/csm_nmr400a_6b9b03a4f0.jpg)
Bruker Avance III HD 400 (‘nmr400a‘)
- Nanobay, installation 2014
- Bruker Ultrashield magnet, installation 2000
- BACS 60 automatic sample changer
- BCU 05 variable temperature precooling unit
- BBFO standard probe with z gradient and ATM, 15N to 31P + 19F / 1H, -150 to +150 °C
Main application:
1D and 2D NMR experiments including heteronuclei
(automation with ICON-NMR software)
![[Translate to Englisch:] Bruker Avance III HD 400 (‘nmr400b‘) [Translate to Englisch:] Bruker Avance III HD 400 (‘nmr400b‘)](/fileadmin/_processed_/9/1/csm_nmr400b_e8c300ddeb.jpg)
Bruker Avance III HD 400 (‘nmr400b‘)
- Nanobay, installation 2013
- Bruker Ascend magnet, installation 2013
- BACS 120 automatic sample changer
- BCU 2 variable temperature precooling unit for sample temperatures down to -60 °C
- Liquid nitrogen heat exchanger for lowest sample temperatures
- BBFO standard probe with z gradient and ATM, 15N to 31P + 19F / 1H, -150 to +150 °C
Main applications:
- 1D and 2D NMR experiments including heteronuclei
(automation with ICON-NMR software) - Variable temperature measurements
Spare probe for 400 MHz (purchase 2001):
BBO with z gradient and ATM, 15N to 31P / 1H